![]() ![]() The initial version, available for the cost of a few clicks, is available here.now! Version 1.15 of the tutorial contains over 100 PowerPoint 'slides', as well as a few external links.Ĭonnection to the internet is not required to use the tutorial, as most of the links are included with the distribution. In the long term, the tutorial will introduce the student to basic procedures, with branches to many 'HOWTOs', Apex2 quick tricks, and more branches to special topics, reaching its ultimate state of production and pedagogy with worked examples of twinning, difficult-to-index crystals, novel integration techniques, and more. Thus: an Apex2 tutorial was conceived and began to slowly move forward. When I last taught my 'X-ray course' here nearly three years ago, it became apparent that a method of self-instruction in diffractometry was sorely needed. The tutorial is a based on a logical progression of successful ideas that began with our popular, and continued with, our X-ray laboratory tutorial for high-school and first-year college students. Many laboratories have Bruker X-ray diffraction instruments running the Apex2 data collection, processing and analysis software. ![]() Since 1913, using the techniques of X-ray Structure Determination, crystallographers have collected data on, and solved, the structures of over 500,000 compounds!!! This tutorial was written with the education of graduate and undergraduate science students in mind, but with the idea of expert mode enhancements at a later time. ![]() The instrument is located in 1709 Gilman Hall. Most of the time it will be equipped with Cu radiation, however, it can be switched to Mo-radiation if needed. #Bruker apex software softwareCurrently we are upgrading it with video camera, modern APEX II Software Suite and low-temperature BRUKER LT-3 device. Chemical shifts are in parts per million using the residual solvent peak (DMSO- d.īruker SMART 1000 CCD Summary BRUKER 1000 CCD Diffractometer will be the second working device for Single Crystal Structure Determination. 1 H NMR spectra were obtained using a Bruker Avance III 500 MHz spectrometer. #Bruker apex software manualThis manual is based on an instrument and software as manufactured around the year 2013. It is intended as a “walk-through” user guide geared especially. The following is guide for collecting data and solving structures using a Bruker APEX II single crystal diffractometer.
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